HCID 21315878, compound → HCID 21315887, compound

HRID 236794Notes

Reaction equation

HRID 236794 reaction equation
[CH3:1][N:2]([CH3:20])[C:3](=O)[CH:4]([S:11][C:12]1[CH:17]=[CH:16][C:15]([CH3:18])=[CH:14][CH:13]=1)[C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1>C(O)C>[CH3:1][N:2]([CH3:20])[C:3]1[C:13]2[CH:14]=[C:15]([CH3:18])[CH:16]=[CH:17][C:12]=2[S:11][C:4]=1[C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1

Participants

3

Reactant 1

HCID 21315878HCID 21315878, compound

Product 1

HCID 21315887HCID 21315887, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Proceed as in Example 31 starting from the N,N-dimethyl-α-(4-methylphenylthio)-α-phenylacetamide (colourless crystals in cyclohexane, mp 99°-102°). The duration of reaction is 5 hours. 61% of theory of colourless needles, mp 89°-92° (ethanol).

Workup

  1. customThe duration of reaction

Sources & evidence

ORD record
ord-577616eed4fe4674bd55d0326c0d02ff
Source dataset
uspto-grants-1979_06
Patent number
US04157399

Reaction notes

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