HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Alanine, ethyl ester, hydrochloride (1:1) → HCID 67152876, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Alanine, ethyl ester, hydrochloride (1:1) | HCID 2724356 | — |
| Reactant | HCID 86653627 | HCID 86653627 | — |
| Product | HCID 67152876 | HCID 67152876 | — |
Reaction Steps
The compound from example 3 (500 mg) is coupled under the conditions in step 4 of example 3 with alanine ethyl ester hydrochloride (152 mg). The crude product obtained is chromatographed on silica gel using the 7:3:0.2 CH2Cl2/MeOH/AcOH mixture. White solid, 530 mg (88%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08703747B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-d45dea30156a411684fcb7a3b4a508e7 |
| Source note | uspto-grants-2014_04 |