HCID 70116313, compound → HCID 70116003, compound

Participants

Reaction Steps

A solution of 4-nitro-1-pyridin-2-yl-1H-pyrazole-3-carboxylic acid dimethylamide (50 mg, 0.19 mmol) in THF (3 ml) was flushed with argon and treated with Pd/C 10% (11 mg, 0.01 mmol). The reaction vessel was evacuated and flushed with hydrogen three times and the reaction was stirred at ambient temperature overnight. The reaction mixture was filtrated and the solvent was evaporated to yield a solid material (44 mg, 99%) which was used without further purification.

Provenance & Evidence