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HRID2368594

反应详情

EQUATION

反应方程式

HRID 2368594 的结构方程式

REACTANTS

反应物

1
结构：CCCCCn1/c(=N/N=C/CCC(=O)O)[nH]c(=O)c2[nH]cnc21
HCID178446142

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCn1c2nc[nH]c2c(=O)n2c(CCC(=O)O)nnc12
HCID57600303

未命名化合物

收率 99%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

The mixture of (4E)-4-[(2E)-(6-oxo-3-pentyl-1,3,6,7-tetrahydro-2H-purin-2-ylidene)hydrazono]butanoic acid (1.367 g, 5.1 mmol) in acetic acid (70 ml) was refluxed for 1 hour. Evaporation of solvent afforded the desired product (1.29 g, 99%) as yellowish solid. LCMS calculated for C14H19N6O3 (M+H): 319.2. Found: 319.2.

WORKUP

后处理

  1. temperaturewas refluxed for 1 hour
  2. customEvaporation of solvent