3,5-Dichlorophenyl isocyanate → HCID 52912059, compound

HRID 2368695Notes

Reaction equation

HRID 2368695 reaction equation
[NH:1]([C:3]1[CH:12]=[C:11]([CH:13]([CH3:15])[CH3:14])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[N:4]=1)[NH2:2].[Cl:16][C:17]1[CH:18]=[C:19]([N:24]=[C:25]=[O:26])[CH:20]=[C:21]([Cl:23])[CH:22]=1>>[Cl:16][C:17]1[CH:18]=[C:19]([NH:24][C:25]([NH:2][NH:1][C:3]2[CH:12]=[C:11]([CH:13]([CH3:15])[CH3:14])[C:10]3[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=3)[N:4]=2)=[O:26])[CH:20]=[C:21]([Cl:23])[CH:22]=1

Participants

3

Reactant 2

HCID 944603,5-Dichlorophenyl isocyanateHCID 67083086HCID 67083086, compound

Product 1

HCID 52912059HCID 52912059, compound

Procedure

A solution of 2-hydrazinyl-4-isopropylquinoline (97 mg, 0.48 mmol) and 91 mg (1.0 eq) of 3,5-dichlorophenyl isocyanate was reacted as outlined in Scheme 1 above to give the desired title compound.

Sources & evidence

ORD record
ord-94910222fbd24beab1c0d97e4566add2
Source dataset
uspto-grants-2014_04
Patent number
US08703797B2

Reaction notes

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