Acetohydrazide → HCID 21315322, compound

HRID 236902Notes

Reaction equation

HRID 236902 reaction equation
[CH2:1]([N:4]=[C:5]=[O:6])[CH:2]=[CH2:3].[C:7]([NH:10][NH2:11])(=[O:9])[CH3:8]>C1C=CC=CC=1>[C:7]([NH:10][NH:11][C:5]([NH:4][CH2:1][CH:2]=[CH2:3])=[O:6])(=[O:9])[CH3:8]

Participants

4

Reactant 2

HCID 14039AcetohydrazideHCID 15123Allyl isocyanate

Product 1

HCID 21315322HCID 21315322, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

Allyl isocyanate (25 g, 0.30 mol) was added slowly to a boiling solution of acethydrazide (22.2 g, 0.30 mol) in dry benzene (300 ml). The mixture was heated for 1 hour whereupon 2 layers formed. The benzene was then evaporated off and the residue triturated with ether to yield the title compound as a white solid. (m.p. 71°-74° C.).

Workup

  1. temperatureThe mixture was heated for 1 hour whereupon 2 layers
  2. customformed
  3. customThe benzene was then evaporated off
  4. customthe residue triturated with ether

Sources & evidence

ORD record
ord-323600ed4d174f68bfdd19af86718314
Source dataset
uspto-grants-1979_06
Patent number
US04158659

Reaction notes

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