HCID 86672620, compound → HCID 86672619, compound

HRID 2369272Notes

Reaction equation

HRID 2369272 reaction equation
[CH3:1][C:2]([CH2:16][CH2:17][CH2:18][CH:19]([CH3:31])[CH2:20][CH2:21][CH2:22][CH:23]([CH3:30])[CH2:24][CH2:25][CH2:26][CH:27]([CH3:29])[CH3:28])=[CH:3][CH2:4][CH2:5][C:6]([O:8][CH2:9][C@@H:10]([C@@H:12]([CH2:14][OH:15])[OH:13])[OH:11])=[O:7]>O>[CH3:1][C:2]([CH2:16][CH2:17][CH2:18][CH:19]([CH3:31])[CH2:20][CH2:21][CH2:22][CH:23]([CH3:30])[CH2:24][CH2:25][CH2:26][CH:27]([CH3:29])[CH3:28])=[CH:3][CH2:4][CH2:5][C:6]([O:8][CH2:9][C@@H:10]([C@@H:12]([CH2:14][OH:15])[OH:13])[OH:11])=[O:7].[OH2:7]

Participants

3

Reactant 1

HCID 86672620HCID 86672620, compound

Product 1

HCID 86672619HCID 86672619, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

mono-O-(5,9,13,17-tetramethyloctadec-4-enoyl)erythritol synthesized in Example 2 and water were homogenously mixed in accordance with the same procedure as in Example 13 to obtain a sample of mono-O-(5,9,13,17-tetramethyloctadec-4-enoyl)erythritol/water system. SAXS analysis of the sample of mono-O-(5,9,13,17-tetramethyloctadec-4-enoyl)erythritol/water system was performed in the same manner as in Example 13. As a result, at least 3 sharp scattering peaks were observed. The peak value ratio exhibited the following ratio peculiar to the reverse hexagonal liquid crystal: 1:√3:2.

Sources & evidence

ORD record
ord-670475ef75fd43aab3404a342d68efed
Source dataset
uspto-grants-2014_04
Patent number
US08703922B2

Reaction notes

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