HCID 75995693, compound → HCID 131731338, compound

HRID 2369273Notes

Reaction equation

HRID 2369273 reaction equation
[CH3:1][C:2]([CH2:16][CH2:17][CH2:18][CH:19]([CH3:31])[CH2:20][CH2:21][CH2:22][CH:23]([CH3:30])[CH2:24][CH2:25][CH2:26][CH:27]([CH3:29])[CH3:28])=[CH:3][CH2:4][CH2:5][CH2:6][O:7][CH2:8][C:9]([CH2:14][OH:15])([CH2:12][OH:13])[CH2:10][OH:11]>O>[CH3:1][C:2]([CH2:16][CH2:17][CH2:18][CH:19]([CH3:31])[CH2:20][CH2:21][CH2:22][CH:23]([CH3:30])[CH2:24][CH2:25][CH2:26][CH:27]([CH3:29])[CH3:28])=[CH:3][CH2:4][CH2:5][CH2:6][O:7][CH2:8][C:9]([CH2:12][OH:13])([CH2:14][OH:15])[CH2:10][OH:11].[OH2:7]

Participants

3

Reactant 1

HCID 75995693HCID 75995693, compound

Product 1

HCID 131731338HCID 131731338, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Mono-O-(5,9,13,17-tetramethyloctadec-4-enyl)pentaerythritol and water were homogeneously mixed in accordance with the same procedure as in Example 13 to obtain a sample of mono-O-(5,9,13,17-tetramethyloctadec-4-enyl)pentaerythritol/water system. SAXS analysis of the sample of mono-O-(5,9,13,17-tetramethyloctadec-4-enyl)pentaerythritol/water system was performed in the same manner as in Example 13. As a result, at least 3 sharp scattering peaks were observed. The peak value ratio exhibited the following ratio peculiar to the reverse hexagonal liquid crystal: 1:√{square root over (3)}:2.

Sources & evidence

ORD record
ord-a2b44acc0feb4899a524cd8bbfe7c282
Source dataset
uspto-grants-2014_04
Patent number
US08703922B2

Reaction notes

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