HCID 86672624, compound → HCID 86672623, compound

HRID 2369275Notes

Reaction equation

HRID 2369275 reaction equation
[CH3:1][C:2]([CH2:15][CH2:16][CH2:17][CH:18]([CH3:30])[CH2:19][CH2:20][CH2:21][CH:22]([CH3:29])[CH2:23][CH2:24][CH2:25][CH:26]([CH3:28])[CH3:27])=[CH:3][CH2:4][CH2:5][CH2:6][O:7][C@H:8]([C@@H:11]([CH2:13][OH:14])[OH:12])[CH2:9][OH:10]>O>[CH3:1][C:2]([CH2:15][CH2:16][CH2:17][CH:18]([CH3:30])[CH2:19][CH2:20][CH2:21][CH:22]([CH3:29])[CH2:23][CH2:24][CH2:25][CH:26]([CH3:28])[CH3:27])=[CH:3][CH2:4][CH2:5][CH2:6][O:7][C@H:8]([C@@H:11]([CH2:13][OH:14])[OH:12])[CH2:9][OH:10].[OH2:7]

Participants

3

Reactant 1

HCID 86672624HCID 86672624, compound

Product 1

HCID 86672623HCID 86672623, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

2-O-(5,9,13,17-tetramethyloctadec-4-enyl)erythritol and water were homogeneously mixed in accordance with the same procedure as in Example 13 to obtain a sample of 2-O-(5,9,13,17-tetramethyloctadec-4-enyl)erythritol/water system. SAXS analysis of the sample of 2-O-(5,9,13,17-tetramethyloctadec-4-enyl)erythritol/water system was performed in the same manner as in Example 13. As a result, at least 4 sharp scattering peaks were observed. The peak value ratio exhibited the following ratio peculiar to the cubic liquid crystal belonging to the crystallographic space group Pn3m: √{square root over (2)}: √{square root over (3)}: √{square root over (4)}: √{square root over (6)}: √{square root over (8)}: √{square root over (9)}.

Sources & evidence

ORD record
ord-bb013c653a084d03a99939b24c4fb6ca
Source dataset
uspto-grants-2014_04
Patent number
US08703922B2

Reaction notes

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