HCID 123603665, compound → HCID 131731352, compound
Reaction equation
[CH3:1][C:2]([CH2:13][CH2:14][CH2:15][CH:16]([CH3:23])[CH2:17][CH2:18][CH2:19][CH:20]([CH3:22])[CH3:21])=[CH:3][CH2:4][C:5]([O:7][CH2:8][CH:9]([CH2:11][OH:12])[OH:10])=[O:6]>O>[CH3:1][C:2]([CH2:13][CH2:14][CH2:15][CH:16]([CH3:23])[CH2:17][CH2:18][CH2:19][CH:20]([CH3:22])[CH3:21])=[CH:3][CH2:4][C:5]([O:7][CH2:8][CH:9]([CH2:11][OH:12])[OH:10])=[O:6].[OH2:6]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
Mono-O-(4,8,12-trimethyltridec-3-enoyl)glycerol synthesized in Example 120 and water were homogeneously mixed in accordance with the same procedure as in Example 13 to obtain a sample of mono-O-(4,8,12-trimethyltridec-3-enoyl)glycerol/water system. SAXS analysis of the sample of mono-O-(4,8,12-trimethyltridec-3-enoyl)glycerol/water system was performed in the same manner as in Example 13. As a result, scattering peaks were observed. The peak value ratio exhibited the following ratio peculiar to the cubic liquid crystal belonging to the crystallographic space group Pn3m: √{square root over (2)}:√{square root over (3)}:√{square root over (4)}.
Sources & evidence
- ORD record
- ord-4fafc42636854b00b30599b94e30a0b3
- Source dataset
- uspto-grants-2014_04
- Patent number
- US08703922B2
Reaction notes
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