HCID 86672624, compound → HCID 123603665, compound

HRID 2369320Notes

Reaction equation

[CH3:1][C:2]([CH2:13][CH2:14][CH2:15][CH:16]([CH3:23])[CH2:17][CH2:18][CH2:19][CH:20]([CH3:22])[CH3:21])=[CH:3][CH2:4][C:5]([O:7][CH2:8][CH:9]([CH2:11][OH:12])[OH:10])=[O:6].O.CC(CCCC(C)CCCC(C)CCCC(C)C)=CCCCO[C@H]([C@@H](CO)O)CO>>[CH3:1][C:2]([CH2:13][CH2:14][CH2:15][CH:16]([CH3:23])[CH2:17][CH2:18][CH2:19][CH:20]([CH3:22])[CH3:21])=[CH:3][CH2:4][C:5]([O:7][CH2:8][CH:9]([CH2:11][OH:12])[OH:10])=[O:6]

Participants

Reactant 2

HCID 86672624HCID 86672624, compound

HCID 131731352HCID 131731352, compound

Product 1

HCID 123603665HCID 123603665, compound

Procedure

Mono-O-(4,8,12-trimethyltridec-3-enoyl)glycerol synthesized in Example 120 and water were homogeneously mixed in accordance with the same procedure as in Example 13 to obtain a sample of mono-O-(4,8,12-trimethyltridec-3-enoyl)glycerol/water system. SAXS analysis of the sample of mono-O-(4,8,12-trimethyltridec-3-enoyl)glycerol/water system was performed in the same manner as in Example 13. As a result, scattering peaks were observed. The peak value ratio exhibited the following ratio peculiar to the cubic liquid crystal belonging to the crystallographic space group Pn3m: √{square root over (2)}:√{square root over (3)}:√{square root over (4)}.

Sources & evidence

ORD record: ord-31728b0bcf304e4cbfdee80998848a6c
Source dataset: uspto-grants-2014_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08703922B2

Reaction notes

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