HCID 86672624, compound → HCID 75995747, compound

HRID 2369324Notes

Reaction equation

[CH3:1][C:2]([CH2:12][CH2:13][CH2:14][CH:15]([CH3:22])[CH2:16][CH2:17][CH2:18][CH:19]([CH3:21])[CH3:20])=[CH:3][C:4]([O:6][CH2:7][CH:8]([CH2:10][OH:11])[OH:9])=[O:5].O.CC(CCCC(C)CCCC(C)CCCC(C)C)=CCCCO[C@H]([C@@H](CO)O)CO>>[CH3:1][C:2]([CH2:12][CH2:13][CH2:14][CH:15]([CH3:22])[CH2:16][CH2:17][CH2:18][CH:19]([CH3:21])[CH3:20])=[CH:3][C:4]([O:6][CH2:7][CH:8]([CH2:10][OH:11])[OH:9])=[O:5]

Participants

Reactant 2

HCID 86672624HCID 86672624, compound

HCID 131731354HCID 131731354, compound

Product 1

HCID 75995747HCID 75995747, compound

Procedure

Mono-O-(3,7,11-trimethyldodec-2-enoyl)glycerol synthesized in Example 146 and water were homogeneously mixed in accordance with the same procedure as in Example 13 to obtain a sample of mono-O-(3,7,11-trimethyldodec-2-enoyl)glycerol/water system. SAXS analysis of the sample of mono-O-(3,7,11-trimethyldodec-2-enoyl)glycerol/water system was performed in the same manner as in Example 13. As a result, scattering peaks were observed. The peak value ratio exhibited the following ratio peculiar to the cubic liquid crystal belonging to the crystallographic space group Pn3m: √{square root over (2)}:√{square root over (3)}:√{square root over (4)}.

Sources & evidence

ORD record: ord-8d844fc7de2c4f70bf148aefaa57824c
Source dataset: uspto-grants-2014_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08703922B2

Reaction notes

Loading…