Allyl bromide → HCID 20304530, compound

HRID 236959Notes

Reaction equation

HRID 236959 reaction equation
[OH:1][C:2]1[C:11]([C:12](=[O:15])[CH2:13][CH3:14])=[CH:10][C:9]2[CH2:8][CH2:7][CH2:6][CH2:5][C:4]=2[CH:3]=1.[CH2:16](Br)[CH:17]=[CH2:18]>>[CH2:18]([O:1][C:2]1[C:11]([C:12](=[O:15])[CH2:13][CH3:14])=[CH:10][C:9]2[CH2:8][CH2:7][CH2:6][CH2:5][C:4]=2[CH:3]=1)[CH:17]=[CH2:16]

Participants

3

Reactant 2

HCID 7841Allyl bromideHCID 20304531HCID 20304531, compound

Product 1

HCID 20304530HCID 20304530, compoundYield 108.4%

Procedure

The product of step (b) (14.5 g) was treated with allyl bromide (11.5 g) under the conditions of Example 1(a) to give the title compound (18.8 g) as a pale brown oil, whose structure was confirmed by MS and NMR spectroscopy.

Sources & evidence

ORD record
ord-c46aa2c59a69423a9a84b93b1a46b1cd
Source dataset
uspto-grants-1979_06
Patent number
US04159273

Reaction notes

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