HuagongsheHuagongshe Chemistry Print Report · For research reference only
Furoin → HCID 178527844, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Furoin | HCID 11100 | — |
| Reactant | Ammonium thiocyanate | HCID 15666 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178527844 | HCID 178527844 | 49.1% |
Reaction Steps
α-Furoin (19.2 g; 0.1 mole) was reacted with 11.5 g (0.15 mole) ammonium thiocyanate in ethanol heated at reflux to afford 11.4 g of 4,5-bis-(2-furyl)-1H-2-imidazolethiol. An analytical sample was prepared by chromatography on alumina with ethanol and recrystallization from nitromethane, m.p. 279°-380° (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04159338 |
| Source dataset | uspto-grants-1979_06 |
| ORD ID | ord-65eab635b120478aa7c2e0cef350716f |
| Source note | uspto-grants-1979_06 |