3-Amino-4-methoxybenzoic acid → HCID 86655912, compound

HRID 2370456Notes

Reaction equation

HRID 2370456 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][C:10]=1[O:11][CH3:12])[C:5]([OH:7])=O.[CH3:13][O:14][C:15]1[CH:16]=[C:17]([SH:25])[CH:18]=[C:19]([O:23][CH3:24])[C:20]=1[O:21][CH3:22]>>[NH2:1][C:2]1[CH:3]=[C:4]([C:5](=[O:7])[S:25][C:17]2[CH:16]=[C:15]([O:14][CH3:13])[C:20]([O:21][CH3:22])=[C:19]([O:23][CH3:24])[CH:18]=2)[CH:8]=[CH:9][C:10]=1[O:11][CH3:12]

Participants

3

Reactant 2

HCID 178233-Amino-4-methoxybenzoic acidHCID 151982403,4,5-Trimethoxybenzenethiol

Product 1

HCID 86655912HCID 86655912, compoundYield 47%

Procedure

Using 3-amino-4-methoxybenzoic acid and 3,4,5-trimethoxyphenylmercaptan as materials, compound 5 is synthesized following a similar method as in Example 28. Yield: 47%.

Sources & evidence

ORD record
ord-52c99d423c7b4386abb48c3d75357544
Source dataset
uspto-grants-2014_04
Patent number
US08710098B2

Reaction notes

Loading…