3,5-Dimethoxyaniline → HCID 67320712, compound

HRID 2370457Notes

Reaction equation

HRID 2370457 reaction equation
[CH3:1][NH:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[C:6]([OH:8])=O.[CH3:14][O:15][C:16]1[CH:17]=[C:18]([CH:20]=[C:21]([O:23][CH3:24])[CH:22]=1)[NH2:19]>>[CH3:24][O:23][C:21]1[CH:20]=[C:18]([NH:19][C:6](=[O:8])[C:5]2[CH:9]=[CH:10][C:11]([O:12][CH3:13])=[C:3]([NH:2][CH3:1])[CH:4]=2)[CH:17]=[C:16]([O:15][CH3:14])[CH:22]=1

Participants

3

Reactant 2

HCID 663013,5-DimethoxyanilineHCID 229768404-Methoxy-3-(methylamino)benzoic acid

Product 1

HCID 67320712HCID 67320712, compoundYield 50%

Procedure

Using 3-methylamino-4-methoxybenzoic acid and 3,5-dimethoxyaniline as materials, compound 40 is synthesized following a similar method as in Example 28. Yield: 50%.

Sources & evidence

ORD record
ord-d172307236f849628db41426faf6808e
Source dataset
uspto-grants-2014_04
Patent number
US08710098B2

Reaction notes

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