HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichlorophenyl isocyanate → HCID 54214036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichlorophenyl isocyanate | HCID 7607 | — |
| Reactant | HCID 2753399 | HCID 2753399 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 54214036 | HCID 54214036 | — |
Reaction Steps
Four and one-tenth grams of m-amino trifluoro acetanilide is dissolved in 100 ml of acetone and 3.8 g. of 3,4-dichlorophenyl isocyanate is added. The mixture is heated to reflux and crystallizes from acetone on cooling. Yield is 6.4 g., m.p. 221°-223° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04159344 |
| Source dataset | uspto-grants-1979_06 |
| ORD ID | ord-39729c125abb496a8fd2b80242a21ad5 |
| Source note | uspto-grants-1979_06 |