HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichlorophenyl isocyanate → HCID 54215760, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichlorophenyl isocyanate | HCID 7607 | — |
| Reactant | HCID 53939566 | HCID 53939566 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 54215760 | HCID 54215760 | — |
Reaction Steps
Five and one-tenth grams of m-amino pentafluoropropionanilide is dissolved in 50 ml of acetone and 3.8 g. of 3,4-dichlorophenyl isocyanate is added. The mixture is heated to reflux, cooled and the acetone stripped off under vacuum. Yield is 8.8 g., m.p. 195°-197° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04159344 |
| Source dataset | uspto-grants-1979_06 |
| ORD ID | ord-3469e82fd43f4e94af3037b142c2a7f0 |
| Source note | uspto-grants-1979_06 |