HCID 46947540, compound → HCID 46944757, compound

HRID 2370585Notes

Reaction equation

CC1(C)N(CCCCCCCCCS(CCCC(F)(F)C(F)(F)F)=[O:17])C(=O)N(C2C=CC([N+]([O-])=O)=C(C(F)(F)F)C=2)C1=O.[CH3:44][C:45]1([CH3:81])[N:49]([CH2:50][CH2:51][CH2:52][CH2:53][CH2:54][S:55][CH2:56][CH2:57][CH2:58][C:59]([F:65])([F:64])[C:60]([F:63])([F:62])[F:61])[C:48](=[O:66])[N:47]([C:67]2[CH:72]=[CH:71][C:70]([N+:73]([O-:75])=[O:74])=[C:69]([C:76]([F:79])([F:78])[F:77])[CH:68]=2)[C:46]1=[O:80]>>[CH3:44][C:45]1([CH3:81])[N:49]([CH2:50][CH2:51][CH2:52][CH2:53][CH2:54][S:55]([CH2:56][CH2:57][CH2:58][C:59]([F:64])([F:65])[C:60]([F:63])([F:62])[F:61])=[O:17])[C:48](=[O:66])[N:47]([C:67]2[CH:72]=[CH:71][C:70]([N+:73]([O-:75])=[O:74])=[C:69]([C:76]([F:79])([F:78])[F:77])[CH:68]=2)[C:46]1=[O:80]

Participants

Reactant 2

HCID 46947540HCID 46947540, compound

HCID 46947724HCID 46947724, compound

Product 1

HCID 46944757HCID 46944757, compound

Procedure

The experimental protocol used is the same as that described for the synthesis of the compound of Example 2, the compound of Example 4 replacing the compound of Example 1. 136 mg of a white solid is obtained (73%). Melting point: 95-96° C.

Sources & evidence

ORD record: ord-d2b063211f9147f8bcd8286dffc556c4
Source dataset: uspto-grants-2014_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08710091B2

Reaction notes

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