HCID 46947540, compound → HCID 46947721, compound

HRID 2370589Notes

Reaction equation

HRID 2370589 reaction equation
[CH3:1][C:2]1([CH3:43])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19][CH2:20][C:21]([F:27])([F:26])C(F)(F)F)=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-:37])=[O:36])=[C:31]([C:38]([F:41])([F:40])[F:39])[CH:30]=2)[C:3]1=[O:42].CC1(C)N(CCCCCCCCCSCCCC(F)(F)[F:64])C(=O)N(C2C=CC([N+]([O-])=O)=C(C(F)(F)F)C=2)C1=O>>[CH3:43][C:2]1([CH3:1])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19][CH2:20][C:21]([F:27])([F:64])[F:26])=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-:37])=[O:36])=[C:31]([C:38]([F:40])([F:41])[F:39])[CH:30]=2)[C:3]1=[O:42]

Participants

3

Reactant 2

HCID 46947540HCID 46947540, compoundHCID 46947720HCID 46947720, compound

Product 1

HCID 46947721HCID 46947721, compoundYield 73%

Procedure

The experimental protocol used is the same as that described for the synthesis of the compound of Example 2, the compound of Example 12 replacing the compound of Example 1. A pale yellow oil is obtained with a yield of 73% (140 mg).

Workup

  1. customA pale yellow oil is obtained with a yield of 73% (140 mg)

Sources & evidence

ORD record
ord-350ac0f647b44297a99ff8f16af2025d
Source dataset
uspto-grants-2014_04
Patent number
US08710091B2

Reaction notes

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