HCID 46945364, compound → HCID 46945365, compound
Reaction equation
[CH3:1][C:2]1([CH3:43])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19][CH2:20][C:21]([F:27])([F:26])[C:22]([F:25])([F:24])[F:23])=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-:37])=[O:36])=[C:31]([C:38](F)(F)F)[CH:30]=2)[C:3]1=[O:42].CC1(C)N(CCCCCCCCCSCCCC(F)(F)C(F)(F)F)C(=O)N(C2C=CC([N+]([O-])=O)=C(C)C=2)C1=O>>[CH3:1][C:2]1([CH3:43])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19][CH2:20][C:21]([F:26])([F:27])[C:22]([F:25])([F:23])[F:24])=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-:37])=[O:36])=[C:31]([CH3:38])[CH:30]=2)[C:3]1=[O:42]Participants
3
Procedure
The experimental protocol used is the same as that described for the synthesis of the compound of Example 2, the compound of Example 23 replacing the compound of Example 1. A colourless oil is obtained with a yield of 50%.
Workup
- customA colourless oil is obtained with a yield of 50%
Sources & evidence
- ORD record
- ord-d4c1ec68d0d44c359f20e307e69d931c
- Source dataset
- uspto-grants-2014_04
- Patent number
- US08710091B2
Reaction notes
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