HCID 46945366, compound → HCID 46945367, compound

HRID 2370596Notes

Reaction equation

HRID 2370596 reaction equation
[CH3:1][C:2]1([CH3:43])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19][CH2:20][C:21]([F:27])([F:26])[C:22]([F:25])([F:24])[F:23])=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-])=O)=[C:31]([C:38](F)(F)F)[CH:30]=2)[C:3]1=[O:42].NC1C=CC(N2C(=O)C(C)(C)N(CCCCCCCCCSCCCC(F)(F)C(F)(F)F)C2=O)=CC=1C>>[NH2:35][C:32]1[CH:33]=[CH:34][C:29]([N:4]2[C:3](=[O:42])[C:2]([CH3:1])([CH3:43])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19][CH2:20][C:21]([F:26])([F:27])[C:22]([F:25])([F:23])[F:24])=[O:17])[C:5]2=[O:28])=[CH:30][C:31]=1[CH3:38]

Participants

3

Reactant 2

HCID 46945366HCID 46945366, compoundHCID 46947540HCID 46947540, compound

Product 1

HCID 46945367HCID 46945367, compoundYield 56%

Procedure

The experimental protocol used is the same as that described for the synthesis of the compound of Example 2, the compound of Example 25 replacing the compound of Example 1. A colourless oil is obtained with a yield of 56%.

Workup

  1. customA colourless oil is obtained with a yield of 56%

Sources & evidence

ORD record
ord-9ee9407b94d642d89db6750a999d5ebe
Source dataset
uspto-grants-2014_04
Patent number
US08710091B2

Reaction notes

Loading…