3,4,5-Trifluorobenzaldehyde → HCID 59268545, compound

HRID 2370741Notes

Reaction equation

HRID 2370741 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([CH:7]=[C:8]([F:11])[C:9]=1[F:10])[CH:5]=O.[CH3:12][O:13][CH:14]([O:25][CH3:26])[CH2:15][NH:16]CC1C=CC(F)=CC=1>>[CH3:12][O:13][CH:14]([O:25][CH3:26])[CH2:15][NH:16][CH2:5][C:4]1[CH:3]=[C:2]([F:1])[C:9]([F:10])=[C:8]([F:11])[CH:7]=1

Participants

3

Reactant 2

HCID 27769543,4,5-TrifluorobenzaldehydeHCID 11615438N-(2,2-dimethoxyethyl)-N-(4-fluorobenzyl)amine

Product 1

HCID 59268545HCID 59268545, compound

Procedure

Starting from 3,4,5-trifluorobenzaldehyde, the title compound was prepared following the method described for 2,2-dimethoxy-ethyl)-(4-fluoro-benzyl)-amine (3). Rt=0.79 min (Method #4). Detected mass: 250.1 (M+H+).

Sources & evidence

ORD record
ord-9126326f30414b5fa58f9be9e6fbf3bc
Source dataset
uspto-grants-2014_04
Patent number
US08710228B2

Reaction notes

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