HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Acetate → 7-(alpha,alpha,alpha-Trifluoro-m-tolyl)-1,2,4-triazolo[4,3-b]-1,2,4-triazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Acetate | HCID 517045 | — |
| Edukt | 3,4-Diamino-1,2,4-triazole | HCID 567144 | — |
| Edukt | 3-(Trifluoromethyl)phenylglyoxal | HCID 2783284 | — |
| Lösungsmittel | Acetic Acid | HCID 176 | — |
| Produkt | 7-(alpha,alpha,alpha-Trifluoro-m-tolyl)-1,2,4-triazolo[4,3-b]-1,2,4-triazine | HCID 12581259 | — |
Reaktionsschritte
A solution of 12.5 g. of m-trifluoromethylphenylglyoxal, 7.69 g. of 3,4-diamino-4H-1,2,4-triazole and 4.67 g. of sodium acetate in 120 ml. of 67% acetic acid is reacted as described in Example 4, giving the desired product as a yellow solid, m.p. 288°-290° C. (dec.).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04159375 |
| Quelldatensatz | uspto-grants-1979_06 |
| ORD ID | ord-f4851c6324344971a5eec2736d4ea614 |
| Quellennotiz | uspto-grants-1979_06 |