HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12581291, compound → HCID 12581305, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12581291 | HCID 12581291 | — |
| Reactant | Ethylorthoformate | HCID 53630039 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 12581305 | HCID 12581305 | — |
Reaction Steps
A mixture of one gram of 3-hydrazino-6-(α,α,α-trifluoro-m-tolyl)-1,2,4-triazine and 15 ml. of ethyl orthoformate is refluxed for 4 hours, cooled and poured into hexane. The solid is collected by filtration and washed with ethanol giving the desired product, m.p. 229°-232° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04159375 |
| Source dataset | uspto-grants-1979_06 |
| ORD ID | ord-7f75f2bfb0e74628953ca4fa9d309ef6 |
| Source note | uspto-grants-1979_06 |