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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2371105Generated: November 1, 2026

Trifluoroacetic acid → HCID 11853395, compound

https://huagongshe.com/reaction/2371105

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 69245421HCID 69245421—
SolventDichloromethaneHCID 6344—
ProductHCID 11853395HCID 1185339577.6%

Reaction Steps

To a solution of the compound (120 mg) obtained from step 8 above in dichloromethane (5 ml) was added trifluoroacetic acid (2 ml) and stirred the reaction mixture for 2 hours at room temperature. The solvent was evaporated under reduced pressure and the residue thus obtained was purified by preparative thin layer chromatography (eluant: 60% ethyl acetate in hexane) to furnish the title compound (68 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08710261B2
Source datasetuspto-grants-2014_04
ORD IDord-0a588f89edcc44df8d92143a52cc99de
Source noteuspto-grants-2014_04