Hydrochloric Acid → HCID 66671358, compound

Participants

Reaction Steps

Aqueous solution of lithium hydroxide (22 mg) was added to a solution of the compound (120 mg) obtained from Step 1 above, in tetrahydrofuran:methanol:water (3:1:1, 5 ml) and the reaction mixture was stirred overnight. The reaction mixture was concentrated and the residue thus obtained was taken in distilled water, acidified with dilute hydrochloric acid solution and extracted with ethyl acetate. The organic layer was washed with distilled water and brine solution and dried over anhydrous sodium sulphate. The solvent was evaporated under reduced pressure to furnish the title compound (100 mg).

Provenance & Evidence