Sodium borohydride → HCID 11856284, compound

Participants

Reaction Steps

To a solution of the compound (160 mg) obtained from Step 2 above in trifluororacetic acid (2 ml) at room temperature was added sodium borohydride (36 mg) and stirred for 1 h. The volatiles were evaporated under reduced pressure and the residue purified by preparative TLC using 10% methanol-DCM as the mobile phase (100 mg).

Provenance & Evidence