HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178444257, compound → HCID 178444258, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178444257 | HCID 178444257 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178444258 | HCID 178444258 | — |
Reaction Steps
A solution of 1.9 g of 1-(p-ethoxyphenyl)-2-[4'-(trans-4-n-pentylcyclohexyl)-3'-fluorobiphenyl-4-yl]ethene [obtained by Heck coupling of 4-ethoxystyrene with 4'-(trans-4-n-pentylcyclohexyl)-3'-fluoro-4-bromobiphenyl] in 50 ml of tetrahydrofuran is hydrogenated in the presence of Pd/C. Customary work-up gives 1-(p-ethoxyphenyl)-2-[4'-(trans-4-n-pentylcyclohexyl)-3'-fluorobiphenyl-4-yl)ethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05093026 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-2458790558064a8892210fcfb67eadf5 |
| Source note | uspto-grants-1992_03 |