Ethanol → 55141-86-1

HRID 237140Notes

Reaction equation

HRID 237140 reaction equation
[C:1]1(=[O:7])[O:6][C:4](=[O:5])[CH:3]=[CH:2]1.C(=O)([O-])[O-].[Na+:12].[Na+].[CH2:14]([OH:16])[CH3:15]>>[C:4]([O:16][CH2:14][CH3:15])(=[O:5])/[CH:3]=[CH:2]\[C:1]([O-:6])=[O:7].[Na+:12]

Participants

4

Reactant 3

HCID 702EthanolHCID 7923Maleic AnhydrideHCID 10340Sodium Carbonate

Product 1

HCID 2366558855141-86-1

Procedure

Fifty-seven grams (0.57 moles) maleic anhydride is dissolved in 500 mls ethanol. With the aid of a pH meter the pH is adjusted to 8.5-8.6 with sodium carbonate. The solution is evaporated on the roto evaporator and dried in a vacuum oven. Ninety-four grams (0.57 moles) of product having a purity of 99.4% (NMR analysis) is obtained.

Workup

  1. customThe solution is evaporated on the roto evaporator
  2. customdried in a vacuum oven
  3. customis obtained

Sources & evidence

ORD record
ord-77be162e4a17436db85b56f33f9b1a7c
Source dataset
uspto-grants-1979_06
Patent number
US04159388

Reaction notes

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