HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzaldehyde → HCID 19907324, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzaldehyde | HCID 7725 | — |
| Reactant | 4-Fluoroanthranilic acid | HCID 2724967 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19907324 | HCID 19907324 | — |
Reaction Steps
4-Fluoroanthranilic acid (1.0 g) and 4-methylbenzaldehyde (0.77 g) were added to ethanol (100 ml). The mixture was heated under reflux for 6 hours, cooled and evaporated under reduced pressure. The residue was recrystallised from toluene to give 4-fluoro-N-(4-methylbenzylidene)-anthranilic acid, mp 144°-5°. (Compound 13).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05093364 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-09d2d2b57fce4273a6df6f4ca1d57e5b |
| Source note | uspto-grants-1992_03 |