HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromophenacyl bromide → tert-butyl N-[2-(4-bromophenyl)-2-hydroxyethyl]-N-methylcarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromophenacyl bromide | HCID 7454 | — |
| Reactant | tert-Butyl 2-hydroxy-2-(4-morpholin-4-ylphenyl)ethyl(methyl)carbamate | HCID 22574361 | — |
| Product | tert-butyl N-[2-(4-bromophenyl)-2-hydroxyethyl]-N-methylcarbamate | HCID 22574334 | — |
Reaction Steps
As described for the preparation of tert-Butyl 2-hydroxy-2-(4-morpholin-4-ylphenyl)ethyl(methyl)carbamate (Preparations 87-88), 2,4′-dibromoacetophenone was converted to the title compound, isolated as a pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06852731B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-8e56bd0d17494d0eadb3bf291f1a949e |
| Source note | uspto-grants-2005_02 |