11-Bromoundecanoic acid → Methyl 11-bromoundecanoate

HRID 2371515Notes

Reaction equation

HRID 2371515 reaction equation
[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([OH:14])=[O:13].Br[CH2:16]CCCCC(O)=O>>[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([O:14][CH3:16])=[O:13]

Participants

3

Reactant 2

HCID 1781211-Bromoundecanoic acidHCID 202106-Bromohexanoic acid

Product 1

HCID 223913Methyl 11-bromoundecanoateYield 90%

Procedure

12.0 grams (45 mmole) of 11-bromoundecanoic acid was treated in the same manner as described above for 6-bromohexanoic acid to yield greater than 90% methyl 11-bromoundecanoate.

Sources & evidence

ORD record
ord-4c98c9f3d36f4dfc80edf5b2ec14c299
Source dataset
uspto-grants-1992_03
Patent number
US05093471

Reaction notes

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