Ethanol → HCID 19907453, compound

HRID 2371530Notes

Reaction equation

HRID 2371530 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][CH:10]=[CH:11][CH2:12][CH2:13][C:14]([O-:16])=[O:15])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:17](O)[CH3:18]>[Pd]>[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][C:14]([O:16][CH2:17][CH3:18])=[O:15])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 702EthanolHCID 86745534HCID 86745534, compound

Product 1

HCID 19907453HCID 19907453, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

First, 831 mg of et - 8-phenyl-4-octenoate was dissolved in 17 ml of absolute ethanol, and after adding 83 mg of 5% palladium on carbon, the mixture was stirred under a hydrogen gas flow at a room temperature for 80 minutes. After filtering off the catalyst, the filtrate was evaporated to obtain 795 mg of ethyl 8-phenyloctanoate as a colorless liquid.

Workup

  1. filtrationAfter filtering off the catalyst
  2. customthe filtrate was evaporated

Sources & evidence

ORD record
ord-986e5a78dcb54fd382f0ed0aa3178d1b
Source dataset
uspto-grants-1992_03
Patent number
US05093370

Reaction notes

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