Diethylamine → HCID 19907465, compound

Participants

Reaction Steps

First, 0.42 g of 1,4-bis(6-bromohexyl)benzene and 0.44 g of diethylamine were dissolved in 5 ml of absolute ethanol, and the mixture was refluxed for 2 hours. After removing the solvent under a reduced pressure and adding chloroform, the mixture was evaporated under a reduced pressure. The residue was acidified with 1N hydrochloric acid, washed with chloroform, alkalized with 10% sodium hydroxide, subjected to salting out, and extracted with total 80 ml of chloroform. The extract was washed with water and a saturated sodium chloride aqueous solution, dried over magnesium sulfate, and evaporated under a reduced pressure to obtain 0.37 g of the title compound as a pale yellow liquid.

Provenance & Evidence