Ethanol → HCID 19907482, compound

Participants

Reaction Steps

First, 300 mg of 1,4-bis(6-diethylaminohexyl)benzene were dissolved in 3 ml of absolute ethanol, and after adding 616 μl of ethyl iodide, the mixture was stirred at a room temperature for 30 minutes, refluxed for 1.5 hours, and then cooled. The mixture was evaporated under a reduced pressure, and after adding 3 ml of acetone, evaporated under a reduced pressure. The residue was dissolved in 1.5 ml of acetone, and the solution was allowed to stand in a freezer for 2 days. The resulting crystal was collected by filtration, washed with ethyl acetate and dried under a reduced pressure to obtain 490 mg of the title compound as a colorless crystal.

Provenance & Evidence