N-Methylpiperidine → HCID 19907440, compound

Participants

Reaction Steps

First, 0.28 g of 1,4-bis(6-bromohexyl)benzene and 0.5 g of N-methylpiperidine were dissolved in 4 ml of absolute ethanol, and the mixture was refluxed for 2 hours and evaporated under a reduced pressure to remove the solvent. After adding acetone and then ethanol, the whole was allowed to stand in a freezer for 3 days. The resulting crystal was collected by filtration, washed with acetone and dried under a reduced pressure to obtain 0.125 g of the title compound as a colorless crystal.

Provenance & Evidence