Ethanol → HCID 15284073, compound

Participants

Reaction Steps

First, 600 mg of 1,4-bis(6-diethylaminohexyl)-2-nitrobenzene was dissolved in 7 ml of absolute ethanol, and after adding 2.18 g of ethyl iodide at a room temperature with stirring, the mixture was refluxed for 3 hours and then cooled. The reaction mixture was evaporated under a reduced pressure, diluted with 3 ml of acetone, and after adding 1 ml of ethyl acetate allowed to stand in a freezer overnight. Resulting crystal was collected by filtration, washed with acetone/ethyl acetate (1:1), and dried under a reduced pressure to obtain 555 mg of the title compound as a pale yellow crystal.

Provenance & Evidence