HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54102380, compound → HCID 19907483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54102380 | HCID 54102380 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19907483 | HCID 19907483 | 84.1% |
Reaction Steps
First, 707 mg of 1,4-bis(6-ethoxycarbonyl-3-hexenyl)benzene was dissolved in 14 ml of ethanol, and after adding 70 mg of 5% palladium/carbon, the mixture was stirred under hydrogen flow at a room temperature for 2 hours, filtered to remove the catalyst, and concentrated under a reduced pressure to obtain 601 mg of 1,4-bis(6-ethoxycarbonylhexyl)benzene as a colorless liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05093370 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-1034bd9153724693ba9c9f7b4b3d10f1 |
| Source note | uspto-grants-1992_03 |