Diethylamine → HCID 19907346, compound

Participants

Reaction Steps

To a solution of 132 mg of 2,6-bis(3-bromopropyl)naphthalene in 1 ml of absolute ethanol was added dropwise 368 μl of diethylamine at a room temperature with stirring, and the mixture was refluxed for 2.5 hours and then cooled. The reaction mixture was evaporated under a reduced pressure, and after adding 20 ml of water, extracted with 50 ml of benzene. The extract was washed with a saturated sodium chloride aqueous solution, dried over magnesium sulfate, filtered, and evaporated under a reduced pressure to obtain 78 mg of the title compound as a pale yellow liquid.

Provenance & Evidence