Ethanol → HCID 19907471, compound

Participants

Reaction Steps

First, 510 mg of 1,4-bis(5-diethylaminopentylthio)benzene was dissolved in 5 ml of absolute ethanol, and after adding 960 μl of ethyl iodide, the mixture was refluxed for 4 hours, then cooled and evaporated under a reduced pressure to remove the ethanol. After adding 5 ml of acetone, the mixture was stirred at a room temperature for 3 hours and allowed to stand in a freezer overnight. The resulting crystal was collected by filtration, washed with acetone and dried under a reduced pressure to obtain 519 mg of the title compound as a light gray crystal.

Provenance & Evidence