Ethanol → HCID 19907411, compound

Participants

Reaction Steps

To a solution of 223 mg of 1,4-bis(8-diethylaminooctyl)benzene in 1 ml of ethanol was added 0.40 ml of ethyl iodide, and the mixture was refluxed for 2 hours, concentrated under a reduced pressure and further dried under reduced pressure. To the residue was added 3 ml of ethyl acetate to solidify the residue. To the solid was added 3 ml of acetone and the whole was stirred for 10 minutes and filtered. The resulting crystal was washed with ethyl acetate and n-hexane, and dried under a reduced pressure to obtain 315 mg of the title compound as a yellow crystal.

Provenance & Evidence