Acetone → HCID 19907424, compound

Participants

Reaction Steps

To a solution of 95 mg of 1,10-bis(dimethylamino)-4,7-decanedione in 3 ml of methanol was added 36 mg of sodium borohydride with ice-cooling, and the mixture was stirred for an hour, and after adding 5 ml of acetone, concentrated under a reduced pressure. After adding chloroform, the mixture was again concentrated under reduced pressure. After adding 5 ml of chloroform, the mixture was filtered to remove insoluble matter, concentrated under a reduced pressure, and further dried under a reduced pressure to obtain 79 mg of the title compound comprising Syn/Anti (1:1) mixture as a yellow oil.

Provenance & Evidence