HRID2371621

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CCCc1c(OCCCOc2ccc(Cl)cc2)ccc2c1OC(CCC(=O)OCC)(CCC(=O)OCC)CC2=O

HCID15157438

未命名化合物

结构：CCCc1c(OCCCOc2ccc(Cl)c3ccccc23)ccc2c1OC(CCC(=O)OCC)(CCC(=O)OCC)CC2=O

HCID15157451

未命名化合物

PRODUCTS

生成物

结构：CCCc1c(OCCCOc2ccc(Cl)c3ccccc23)ccc2c1OC(CCC(=O)O)(CCC(=O)O)CC2=O

HCID15157452

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

The title compound was prepared by the method of Example 22 substituting the title product of Example 34 (515 mg) for the title product of Example 21 to give, after trituration with diethylether, 352 mg as a solid, m.p. 170.5°-171° C.

WORKUP

后处理

customto give

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-056992e92e1f43abbdec47f98d07f01f
来源数据集: uspto-grants-1992_03
DOI: 10.6084/m9.figshare.5104873.v1
专利: US05093353
来源说明: uspto-grants-1992_03

反应 SMILES

[Cl:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[C:5]([O:12][CH2:13][CH2:14][CH2:15][O:16][C:17]2[CH:41]=[CH:40][C:20]3[C:21](=[O:39])[CH2:22][C:23]([CH2:32][CH2:33][C:34]([O:36]CC)=[O:35])([CH2:25][CH2:26][C:27]([O:29]CC)=[O:28])[O:24][C:19]=3[C:18]=2[CH2:42][CH2:43][CH3:44])=[CH:4][CH:3]=1.ClC1C=CC(OCCCOC2C=CC3C(=O)CC(CCC(OCC)=O)(CCC(OCC)=O)OC=3C=2CCC)=CC=1>C(OCC)C>[Cl:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[C:5]([O:12][CH2:13][CH2:14][CH2:15][O:16][C:17]2[CH:41]=[CH:40][C:20]3[C:21](=[O:39])[CH2:22][C:23]([CH2:32][CH2:33][C:34]([OH:36])=[O:35])([CH2:25][CH2:26][C:27]([OH:29])=[O:28])[O:24][C:19]=3[C:18]=2[CH2:42][CH2:43][CH3:44])=[CH:4][CH:3]=1