HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 18964669, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 19905970 | HCID 19905970 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18964669 | HCID 18964669 | — |
Reaction Steps
36.0 g of the 2-(2-hexyldecyloxy)benzoic acid was dissolved in 100 ml of methylene chloride, 0.5 ml of N,N-dimethylformamide was added, and 13 ml of oxalyl chloride was added dropwise over about 30 min at room temperature with stirring. After the addition the stirring was continued for 2 hours further and it was concentrated, to obtain 2-(2-hexyldecyloxy)benzoic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05094938 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-ad63a2d86bb049efb465f0558a8f6261 |
| Source note | uspto-grants-1992_03 |