2-Allylphenol → HCID 54400586, compound

HRID 2371718Notes

Reaction equation

[CH2:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[OH:10])[CH:2]=[CH2:3].Cl[C:12]1[C:13](Cl)=[C:14]([CH3:19])[CH:15]=[CH:16][C:17]=1[CH3:18]>>[CH:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[O:10][CH2:18][C:17]1[CH:16]=[CH:15][C:14]([CH2:19][O:10][C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[CH:1]=[CH:2][CH3:3])=[CH:13][CH:12]=1)=[CH:2][CH3:3]

Participants

Reactant 2

HCID 156242-Allylphenol

HCID 2867292,3-dichloro-1,4-dimethylbenzene

Product 1

HCID 54400586HCID 54400586, compound

Procedure

α,α'-bis-(ortho-propenylphenoxy)-para-xylene is prepared in a procedure similar to Example I, except that 459.3 grams (3.4 moles) of 2-allylphenol is employed along with 300 grams (1.7 mole) of dichloro-para-xylene to yield 597 grams (95% yield) of a white crystalline solid having a melting point of 50°-53° C.

Sources & evidence

ORD record: ord-c5c6dd13f6bd4eddae873647dc22e25e
Source dataset: uspto-grants-1992_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05095074

Reaction notes

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