HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 13420167, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | 3-[2-(Trifluoromethyl)phenoxy]azetidine | HCID 12812505 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 13420167 | HCID 13420167 | — |
Reaction Steps
To 4.5 g (0.02 mole) of 3-[2-(trifluoromethyl)phenoxy]azetidine stirring in 50 ml of dry benzene, was added slowly 1.2 g (0.02 mole) of methyl isocyanate at room temperature. Stirring was continued for 30 minutes. A solid formed, and after filtration was recrystallized from benzene to yield 3.5 g (68%), mp 134°-136°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05095014 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-1a3a609d96214fbe9589953797d87e93 |
| Source note | uspto-grants-1992_03 |