HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → 3-Phenylammonio-1-propanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Propane sultone | HCID 14264 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 3-Phenylammonio-1-propanesulfonate | HCID 12546060 | 95% |
Reaction Steps
A mixture of aniline (7 mmol) and propane sultone (10 mmol) was heated in 10 mL of acetonitrile at 12.0-130° C. for 9 h in a pressure tube under argon atmosphere. The product was allowed to cool to room temperature and the solid of 3-phenylammonio-1-propanesulfonate was filtered and air-dried. Yield: 95%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642014B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-f03ab8001ee74a3fa69d20bb82c32bc4 |
| Source note | uspto-grants-2014_02 |