HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54323543, compound → 19915-11-8
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54323543 | HCID 54323543 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 19915-11-8 | HCID 12654976 | 104.7% |
Reaction Steps
A solution of the cis-bicyclo ;3.3.0]oct-6-ene-3-one (6.2 g .05 mol) in 150 mL of ethyl acetate containing 0.50 g of 10% Pd/C was hydrogenated at 25 psi for 11/2 hours. The catalyst was removed by filtering through Celite and the solvent evaporated to give 6.5 g of cis-bicyclo[3.3.0]-octane-3-one (100%). TLC (SiO2CH2Cl2) Rf =0.35 (I2, brown ).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05095109 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-1f5f09d30c064706bc4c2a948ab3f02f |
| Source note | uspto-grants-1992_03 |