HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53862937, compound → N-(4-pivaloyloxymethoxycarbonyl-2,4-(R*,R*)-dibenzylbutyryl)-3-aminopropionic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53862937 | HCID 53862937 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-(4-pivaloyloxymethoxycarbonyl-2,4-(R*,R*)-dibenzylbutyryl)-3-aminopropionic acid | HCID 54190453 | — |
Reaction Steps
0.92 g of N-[4-pivaloyloxymethoxycarbonyl-2,4-(R*,R*)-dibenzylbutyryl]-3-aminopropionic acid benzyl ester in 20 ml of ethanol is hydrogenated at atmospheric pressure in the presence of 0.1 g of 5% palladium on carbon. The reaction is filtered and evaporated to give N-(4-pivaloyloxymethoxycarbonyl-2,4-(R*,R*)-dibenzylbutyryl)-3-aminopropionic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05096925 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-d03908ec14f543b5919bd31008f12a49 |
| Source note | uspto-grants-1992_03 |